MS Report from Instrument: LCMS-02 File ..6 2017-06-26 16-02-10\\BIZ2017-626-WYQ12_1.D Tgt Mass (CHM): Injection Date : 26 Jun 17 6:00 pm +0800 Seq. Line : 27 Sample Name : BIZ2017-626-WYQ12_1 Location : P1-E-01 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 0.5 ul Acq. Method : D:\\chem32\\1\\DATA\\20170626\\20170626 2017-06-26 16-02-10\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\DATA\\20170626\\20170626 2017-06-26 16-02-10\\1-POS-3MIN.M Catalog No : HY-W004049 Batch#25067 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 B, Sig=214,4 Ref=off 1.2790.441mAU100050001.4471.4742.0790.5 DAD1 C, Sig=2,4 Ref=off mAU75500.44525011.2791.522.5min1.3181.6941.4511.8272.0710.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 702500020000150001000050001.3031.522.5min0.51 Ion 139, MSD1 139,Target Mass 138 +H Positive, EIC=138.7:139.7 60004000200000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.3051.522.5min1.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.44 0.02 0.99 0.84 0.05 ND 1.28 0.02 13.50 1591.92 99.82 2 1.45 0.02 0.94 0.86 0.05 163 1.47 0.02 0. 0.50 0.03 ND 2.08 0.02 0.97 0.88 0.05 233 Integration Results for DAD1 C, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.45 0.29 0.92 0.68 0.76 163 1.28 0.02 117.22 100.48 96.80 2 1.32 0.02 0.88 1.12 0.73 139 1.45 0.02 0.30 0.28 0.25 163 1.69 0.02 0.47 0.90 0.38 ND 1.83 0.02 0.37 0.32 0.31 233 2.07 0.04 0.93 0.60 0.77 233 Integration Results for MSD1 TIC, MS FileLCMS-02 6/27/2017 9:58:14 CLJ_701Page 1 of 3
MS Report from Instrument: LCMS-02 RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.30 0.09 99849.81 19411. 100.00 2LCMS-02 6/27/2017 9:58:14 CLJ_701Page 2 of 3
MS Report from Instrument: LCMS-02Ret. Time: 1.30 <<<< POSITIVE SPECTRA >>>> ES-API Positive12001000800600 233.0 2.0 169.1 186.1 205.2 129.1 147.1 279.3 327.0 397.0 447.1 520.34002000200300400500600700800900m/z 2.2 163.1 139.1 418.6LCMS-02 6/27/2017 9:58:14 CLJ_701 300.9 349.3 477.2Page 3 of 3
