Chlorphenoxamine_LCMS_19152_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20160107\\20160107 2016-01-07 09-07-04\\BIZ2016-107-WJ2.DSample Name: BIZ2016-107-WJ2=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 20Acq. Instrument : HY-LCMS-02 Location : P2-C-08Injection Date : 1/7/2016 10:44:59 AM Inj : 1 Inj Volume : 3.000 µlDifferent Inj Volume from Sample Entry Actual Inj Volume : 5.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20160107\\20160107 2016-01-07 09-07-04\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 1/7/2016 9:07:05 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20160107\\20160107 2016-01-07 09-07-04\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 1/7/2016 10:58:50 AM by Yang Qian(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-B1607 Batch#19152 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT 1260\\DATA\\20160107\\20160107 2016-01-07 09-07-04\\BIZ2016-107-WJ2.D) 1.719mAU700600500400300 2.0171000-1000.511.5 1.610 2.25620022.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.610 MM 0.0372 5.02337 2.25347 0.1075 2 1.719 MM 0.0987 4585.20361 774.52637 98.0785 3 2.017 MM 0.0583 68.51734 19.59984 1.4656 4 2.256 MM 0.0414 16.283 6.55353 0.3484 Totals : 4675.03325 802.93321 ===================================================================== *** End of Report ***HY-LCMS-02 1/7/2016 10:59:23 AM Yang Qian(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20160107\\20160107 2016-01-07 09-07-04\\BIZ2016-107-WJ2.DSample Name: BIZ2016-107-WJ2=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 20Acq. Instrument : HY-LCMS-02 Location : P2-C-08Injection Date : 1/7/2016 10:44:59 AM Inj : 1 Inj Volume : 3.000 µlDifferent Inj Volume from Sample Entry Actual Inj Volume : 5.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20160107\\20160107 2016-01-07 09-07-04\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 1/7/2016 9:07:05 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20160107\\20160107 2016-01-07 09-07-04\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 1/7/2016 11:00:29 AM by Yang Qian(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-B1607 Batch#19152 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20160107\\20160107 2016-01-07 09-07-04\\BIZ2016-107-WJ2.D) ES-API, Pos, Scan 1.72960000050000040000030000020000010000000.511.522.53min HY-LCMS-02 1/7/2016 11:01:23 AM Yang Qian(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20160107\\20160107 2016-01-07 09-07-04\\BIZ2016-107-WJ2.DSample Name: BIZ2016-107-WJ2MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.729 5657244 306.20 I 305.20 I 304.20 I*MSD1 SPC, time=1.6:1.835 of D:\\AGLIENT 1260\\DATA\\20160107\\20160107 2016-01-07 09-07-04\\BIZ2016-107-WJ2.D ES-API, 100806040200100200300400500600700800m/z 307.2 305.2 306.2 304.2Max: 297906 *** End of Report ***HY-LCMS-02 1/7/2016 11:01:23 AM Yang Qian(LCMS-02) 215.1Page 2 of 2